Gas Chromatography of Some Synthetic Drugs

Statistical Analysis of Some Gas Chromatography Measurements

The National Bureau of Standards has certified Standard Reference Materials (SRMs) for the concentration of polychlorinated biphenyls (PCBs) in hydrocarbon matrices (transformer and motor oils). The certification of these SRMs involved measurements of extremely small concentrations of PCBs made by gas chromatography. Despite the high accuracy of the measurement techmique, the correlated data ca...

Gas--liquid chromatography-mass spectrometry of synthetic ceramides.

Two series of ceramides with either sphingosine (sphing-4-enine) or sphinganine as base and with one of the saturated fatty acids C(16), C(18), C(20), C(22), C(24), C(26), or oleic acid were analyzed as the 1,3-di-O-trimethylsilyl ether derivatives by gas chromatography-mass spectrometry. The fragments formed on electron impact can be divided into three main groups, namely "molecular weight fra...

Gas chromatography of cannabis constituents and their synthetic derivatives.

Identification of volatile organic compounds of some Trichoderma species using static headspace gas chromatography-mass spectrometry

Fungi release wide spectrum of volatile organic compounds (VOCs) that belong to several chemical groups with different biochemical origins such as monoterpenes, sesquiterpenes, alcohols, aldehydes, aromatic compounds, esters, furans, ketones, sulfur and nitrogen compounds. Trichoderma species are the most studied fungal biocontrol agents and are successfully used as biofungicides and biofertili...

Reversed-phase liquid chromatography and gas chromatography/mass fragmentography compared for determination of tricyclic antidepressant drugs.

We compare measurement of the tricyclic antidepressants desipramine, imipramine, nortryptaline, and amitryptaline by reversed-phase "high-performance" liquid chromatography and by gas chromatography/mass fragmentography. The liquid-chromatographic procedure does not require ion-pairing reagents, and involves detection at 215 nm. The within-day and between-day CVs for this method were less than ...